Investigation of processing variables of Ni substrate for YBCO coated conductors

We fabricated cube textured Ni substrates for YBCO coated conductors from the initial specimens prepared by powder metallurgy (P/M) and casting and evaluated the effects of annealing temperature on microstructural evolution and texture formation. To characterize the roles of the two preparation methods, the initial specimens were prepared to be of the same size and experienced the same rolling conditions, and were then annealed in the temperature range of 600°C to 1200°C. The texture was evaluated by X-ray pole-figure analysis and transmission electron microscopy (TEM). The texture analysis indicated that a strong cube texture formed for the substrate made by P/M and this texture did not vary significantly with annealing temperature in the range of 600-1200°C. On the other hand, the texture of the substrate made by casting was more dependent on the annealing temperature, and a twin texture ({221}〈221〉) and several minor texture components began to form at 1000°C. Microstructural observation showed that the morphology of deformation band together with micro-band in the as-rolled tape prepared by P/M was more homogeneous and of higher density than that produced by casting, resulting in a strong cube texture in wider range of annealing temperatures and a finer microstructure after recrystallization.